دانلود کتاب Polymer Chemistry: A Practical Approach

فهرست مطالب :

Cover
Preface
Contents
Contributors
Abbreviations
1. Polymer characterization
1.1. Introduction
1.2. Synthetic routes to polymers
1.3. Molecular weight determination
1.4. Composition and microstructure
1.5. Optical microscopy
1.6. Electron microscopy
1.7. Analytical microscopy
1.8. Scanning probe microscopy
1.9. Thermal analysis
1.10. Molecular relaxation spectroscopy
1.11. X-ray and neutron scattering methods
1.12. Conclusions
References
2. General procedures in chain-growth polymerization
2.1. Introduction
2.2. Free-radical chain polymerization
2.3. Anionic polymerization
2.4. Ring-opening polymerizations initiated by anionic reagents
2.5. Coordination polymers
2.6. Conclusions
References
3. Controlled/‘living’ polymerization methods
3.1. Introduction
3.2. Covalent ‘living’ polymerization: group transfer polymerization
3.3. Controlled free-radical polymerizations mediated by nitroxides
3.4. Controlled free-radical polymerizations: atom transfer free-radical polymerizations (ATRP) and aqueous ATRP
References
4. Step-growth polymerization-basics and development of new materials
4.1. Introduction
4.2. The synthesis of an aromatic polyamide
4.3. Preparation of a main-chain liquid crystalline poly(ester ether) with a flexible side-chain
4.4. Non-periodic crystallization from a side-chain bearing copolyester
4.5. A comparison of melt polymerization of an aromatic di-acid containing an ethyleneglycol spacer with polymerization in a solvent and dispersion in an inorganic medium
References
5. The formation of cyclic oligomers during step-growth polymerization
5.1. Introduction
5.2. Synthesis and extraction of cyclic oligomers of poly(ether ketone)
5.3. Synthesis of some sulfone-linked paracyclophanes from macrocyclic thioethers
5.4. Summary
References
6. The synthesis of conducting polymers based on heterocyclic compounds
6.1. Introduction
6.2. Electrochemical synthesis
6.3. Synthesis of polypyrrole
6.4. Synthesis of polyaniline
6.5. Synthesis of polythiophene
6.6. Conclusions
References
7. Some examples of dendrimer synthesis
7.1. Introduction
7.2. Excess reagent method
7.3. Protection–deprotection method
References
8. New methodologies in the preparation of imprinted polymers
8.1. Introduction
8.2. Sacrificial spacer approach
8.3. Preparation of bacteria-imprinted polymers
References
9. Liquid crystalline polymers
9.1. Introduction
9.2. Synthesis of an acrylate-based liquid crystal polymer
9.3. The hydrosilylation reaction: a useful procedure for the preparation of a variety of side-chain polymers
9.4. Photochemical preparation of liquid crystalline elastomers with a memory of the aligned cholesteric phase
9.5. Defining permanent memory of macroscopic global alignment in liquid crystal elastomers
9.6. Summary
References
Index